聚乙烯醇/壳聚糖季铵盐薄膜的制备及其对黄骨鱼保鲜效果研究
Preparation of Polyvinyl Alcohol/Chitosan Quaternary Ammonium Salt Film and Its Preservation Effect of Yellow Bone Fish
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摘要: 为研究聚乙烯醇/壳聚糖季铵盐(PVA/HACC)薄膜对鱼肉保鲜效果和货架期的影响,先用溶液流延法制备含有0%、1%、2%和3% HACC的PVA薄膜,分别验证其力学和疏水性能。将鱼肉用不同质量分数的PVA/HACC薄膜包裹在4℃下贮藏,每3 d取样测定菌落数并进行感官评价。实验表明,当HACC添加量为2%时,对薄膜的透光率影响较小,此时薄膜的拉伸强度为25.45 MPa,断裂伸长率69.8%,综合力学性能良好;吸水率20.1%,润湿角80.2°,疏水性较好;且其包裹的鱼肉在第9 d菌落数量为6.84 lg cfu/g,感官评分为8分,相比空白组在第6 d的菌落数量6.41 lg cfu/g,感官评分7.7分,货架期延长了3 d左右,对鱼肉表面菌落有抑制作用,有效维持鱼肉感官品质。Abstract: In order to study the effect of PVA/HACC film on the preservation effect and shelf life of fish,the PVA film containing 0%,1%,2% and 3% HACC was prepared by solution casting method,the mechanics and hydrophobicity performance were verified. The fish meat was wrapped in PVA/HACC film of different mass fractions and stored at 4℃. The number of colonies was sampled every 3 days and sensory evaluation was performed. Experiments showed that when the addition amount of HACC was 2%,the light transmittance of the film was good. Meanwhile,the tensile strength of the film was 25.45 MPa,the elongation at break was 69.8%,so the comprehensive mechanical properties were good. The water absorption rate was 20.1%,the wetting angle was 80.2°,so the hydrophobicity was satisfied. The number of colonies was 6.84 lg cfu/g and the sensory evaluation was 8 points on the 9th day. Compared with the blank group,the number of colonies on the 6th day was 6.41 lg cfu/g,the sensory score was 7.7. So the shelf life was extended by about 3 days. It had obvious antibacterial effect on fish while the sensory quality of the fish was effectively maintained.