江永香姜姜油树脂的GC-MS分析
Analysis of ginger oleoresin in Jiangyong fragrant-ginger by GC-MS
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摘要: 以我国具有特色的江永香姜作为原料,采用石油醚提取江永香姜中姜油树脂,并通过GC-MS定性分析化学成分,用峰面积归一化法检测各化合物的相对百分含量。结果表明,共鉴定出24种主要化合物,占化学成分总提物的87.38%,其中烯烃类占45.67%,酯类占16.02%,烷烃类占5.76%,醇类占9.34%,酚类占4.04%,醛类占4.56%,酸类占1.99%,其中含量在5%以上的有7种,包括β-红没药烯、反-α-香柑油烯、姜黄烯、α-金合欢烯、(Z)-β-法尼烯5种烯烃,还包括棕榈酸甲酯、9-十八烯酸酯两种酯类。Abstract: Jiangyong fragrant-ginger were used as raw material, which was one of the regional characteristics of jiangyong wuxiang in china. The ginger oleoresin of Jiangyong fragrant-ginger were extracted by petroleum ether and the chemical constituents were separated and identified by GC-MS. Then the relative contents in percentage of compounds were determined by peak area normalization method. The results showed that 24major compounds were separated and accounted for 87.38% of the total extractions. The major constituents were identified as olefins 45.67%, esters 16.02%, alkanes 5.76%, alcohols 9.34%, phenols 4.04%, aldehydes4.56% and acids 1.99%. There were 7 kinds of compounds that the contents were more than 5%, 5 kinds olefins (β-bisabolene, anti-α-be-rgamot oil ene, curcumene, α-farnesene, (Z) -β-farnesene) were included, methyl hexadecanoate, 9-octadecenoic acid were also included.